Volume 13,Issue 1,2017 Table of Contents

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  • 1  Microstructure and microwave absorption properties of MWCNTs reinforced magnesium matrix composites fa- briccated by FSP
    CHEN Yu-hua MAO Yu-qing XIE Ji-lin ZHAN Zi-lin YU Liang
    2017, 13(1):1-4. DOI: 10.1007/s11801-017-6237-0
    [Abstract](4201) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    Multiwall carbon nanotubes (MWCNTs) reinforced magnesium matrix (MWCNTs/Mg) composites were successfully fabricated by friction stir processing (FSP). Microstructure and microwave-absorption properties of WCNTs/Mg composites are studied. The results show that with increasing the MWCNTs content to 7.1% in volume fraction, the agglomeration of MWCNTs is found in the WCNTs/Mg composites. The addition of MWCNTs has little effect on microwave-absorption properties. With increasing the frequency from 2 GHz to 18 GHz, the microwave absorption of the composites decreases. Compared with the absorption loss of the MWCNTs, the reflection loss of base material takes the most part of the loss of the microwave, and the increase of the reflection loss can promote electromagnetic shielding properties of the composites. Moreover, the electromagnetic shielding properties of the composites are less than −85 dB in the lower frequency range from 0.1 MHz to 3 GHz. With increasing the content of MWCNTs, the electrical conductivity of the composites is decreased, and the electromagnetic shielding properties is slightly enhanced.
    2  Investigation on refractive index sensing of single silver nanoparticle at tightly focused light illumination
    SHEN Si WANG Xiang-hui SUN Jing-wei FAN Fei CHANG Sheng-jiang
    2017, 13(1):5-9. DOI: 10.1007/s11801-017-6248-x
    [Abstract](3931) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    Based on the generalized Mie theory, refractive index sensing characteristics of single silver nanoparticle respectively illuminated by tightly focused linearly-polarized and radially-polarized light beams are investigated. The spectra for localized surface plasmon resonances (LSPR) under different dielectric environments demonstrate that distinct dipolar and quadrupolar resonances can be always observed for the case of radial polarization, while there is only strong dipolar resonance for the case of linear polarization. The dipolar mode has a higher sensitivity. However, the figure of merit (FOM) for the quadrupolar resonance is much higher than that for the dipolar resonance, because the quadrupolar resonance has a narrower width.
    3  Enhancement of R6G fluorescence by N-type porous silicon deposited with gold nanoparticles
    MO Jia-qing JIANG Jing ZHAI Zhen-gang SHI Fu-gui JIA Zhen-hong
    2017, 13(1):10-12. DOI: 10.1007/s11801-017-6269-5
    [Abstract](3852) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    By the electrochemical anodization method, we achieve the single-layer macroporous silicon on the N-type silicon, and prepare gold nanoparticles with sodium citrate reduction method. Through injecting the gold nanoparticles into the porous silicon by immersion, the fluorescence quenching mechanism of porous silicon influenced by gold nanoparticles is analyzed. Then the macroporous silicon deposited with gold nanoparticles is utilized to enhance the fluorescence of rhodamine 6G (R6G). It is found that when the macroporous silicon is deposited with gold nanoparticles for 6 h, the maximum fluorescence enhancement of R6G (about ten times) can be realized. The N-type porous silicon deposited with gold nanoparticles can be an excellent substrate for fluorescence detection.
    4  A continuously tunable microwave photonic notch filter with complex coefficient based on phase modulation
    XU Dong CAO Ye TONG Zheng-rong YANG Jing-peng
    2017, 13(1):13-15. DOI: 10.1007/s11801-017-6207-6
    [Abstract](3785) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    A continuously tunable microwave photonic notch filter with complex coefficient based on phase modulation is proposed and demonstrated. The complex coefficient is generated using a Fourier-domain optical processor (FD-OP) to control the amplitude and phase of the optical carrier and radio-frequency (RF) phase modulation sidebands. By controlling the FD-OP, the frequency response of the filter can be tuned in the full free spectral range (FSR) without changing the shape and the FSR of the frequency response. The results show that the center frequency of the notch filter can be continuously tuned from 17.582 GHz to 29.311 GHz with FSR of 11.729 GHz. The shape of the frequency response keeps unchanged when the phase is tuned.
    5  Research on optical fiber magnetic field sensors based on multi-mode fiber and spherical structure
    WANG Yan TONG Zheng-rong ZHANG Wei-hua LUAN Pan-pan ZHAO Yue XUE Li-fang
    2017, 13(1):16-20. DOI: 10.1007/s11801-017-6195-6
    [Abstract](4207) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    A magnetic field sensor with a magnetic fluid (MF)-coated intermodal interferometer is proposed and experimentally demonstrated. The interferometer is formed by sandwiching a segment of single mode fiber (SMF) between a segment of multi-mode fiber (MMF) and a spherical structure. It can be considered as a cascade of the traditional SMF-MMF-SMF structure and MMF-SMF-sphere structure. The transmission spectral characteristics change with the variation of applied magnetic field. The experimental results exhibit that the magnetic field sensitivities for wavelength and transmission loss are 0.047 nm/mT and 0.215 dB/mT for the interference dip around 1 535.36 nm. For the interference dip around 1548.41nm, the sensitivities are 0.077 nm/mT and 0.243 dB/mT. Simultaneous measurement can be realized according to the different spectral responses.
    6  A six-junction GaAs laser power converter with different sizes of active aperture
    SUN Yu-run DONG Jian-rong HE Yang ZHAO Yong-ming YU Shu-zhen XUE Ji-ping XUE Chi WANG Jin LU Yun-qing DING Yan-wen
    2017, 13(1):21-24. DOI: 10.1007/s11801-016-6193-8
    [Abstract](3955) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    We investigate a novel GaAs-based laser power converters (LPCs) grown by metal-organic chemical vapor deposition (MOCVD), which uses a single monolithic structure with six junctions connected by tunnel junctions to obtain a high output voltage. The LPCs with diameters of active aperture of 2 mm and 4 mm were fabricated and tested. The test results show that under an 808 nm laser, two LPCs both show an open circuit voltage of above 6.5 V. A maximum power conversion efficiency of 50.2% is obtained by 2 mm sample with laser power of 0.256 W, and an output electric power of 1.9 W with laser power of 4.85 W is obtained by 4 mm sample. The performances of the LPCs are deteriorated under illumination of high flux, and the 4 mm sample shows a higher laser power tolerance.
    7  Refractive index insensitive temperature sensor based on waist-enlarged few mode fiber bitapers
    LIU Qiang WANG Si-wen FU Xing-hu FU Guang-wei JIN Wa BI Wei-hong
    2017, 13(1):25-28. DOI: 10.1007/s11801-017-6200-0
    [Abstract](3921) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    A refractive index insensitive temperature sensor based on waist-enlarged few mode fiber (FMF) bitapers is presented. The first section of FMF is spliced between two single-mode fibers. In fusion process, the waist-enlarged FMF bitapers can be obtained by large current discharging repeatedly. The refractive index and temperature sensing mechanisms are analyzed. For the sensors with different sizes, the refractive index and temperature experiments have been performed. The results show that in the refractive index ranges of 1.335 0—1.346 6 and 1.348 2—1.419 3, the refractive index insensitivity is verified. In a temperature range of 31.9—90 °C, the sensor sensitivity can be up to 85.57 pm/°C. In addition, it has a compact structure. Therefore, the sensor can avoid the cross sensitivity for measuring the refractive index and temperature simultaneously.
    8  Enhanced efficiency and brightness in organic light- emitting devices with MoO3 as hole-injection layer
    YANG Hui-shan WU Li-shuang
    2017, 13(1):29-32. DOI: 10.1007/s11801-017-6215-6
    [Abstract](3862) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    The organic light-emitting devices (OLEDs) using 4,4’,4’’-tris{N-(3-methylphenyl)-N-phenylamin}triphenylamine (m-MTDATA) and MoO3 or 1,3,5-triazo-2,4,6-triphosphorine-2,2,4,4,6,6-tetrachloride (TAPC) and MoO3 as the hole-injection layer (HIL) were fabricated. MoO3 can be expected to be a good injection layer material and thus enhance the emission performance of OLED. The highest occupied molecular (HOMO) of MoO3 is between those of m-MTDATA or TAPC and N,N’-bis-(1-naphthyl)-N,N’-diphenyl-1,1’-biphenyl-4,4’-diamine (NPB), which reduces the hole-injection barrier and improves the luminance of the OLEDs. The current efficiency is improved compared with that of the device without the MoO3 layer. The highest luminous efficiency of the device with 2-nm-thick MoO3 as HIL is achieved as 5.27 cd/A at 10 V, which is nearly 1.2 times larger than that of the device without it. Moreover, the highest current efficiency and power efficiency of the device with the structure indium-tin oxide (ITO)/TAPC (40 nm)/MoO3 (2 nm)/TcTa:Ir(ppy)3 (10%, 10 nm)/ tris-(8-hydroxyquinoline) aluminium (Alq) (60 nm)/LiF (1 nm)/Al are achieved as 37.15 cd/A and 41.23 lm/W at 3.2 V and 2.8 V, respectively.
    9  Design and fabrication of a sub-millimeter multi-beam folded waveguide structure
    YAN Sheng-mei SU Wei ZHANG Guo-liang
    2017, 13(1):33-37. DOI: 10.1007/s11801-017-6220-9
    [Abstract](3998) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    A novel multi-beam folded waveguide (MBFW) circuit, which can enhance the output power and interaction efficiency of sub-terahertz (THz) traveling wave tube (TWT), is presented in the paper. Operating with fundamental mode and multiple electron beams means that a larger beam current can be used for a higher output power. The characteristics of the MBFW structure are analyzed and optimized. Compared with the single-beam folded waveguide (SBFW) TWT, the output power of the MBFW TWT increases from 3.64 W to 25.45 W at 140 GHz and its electronic efficiency increases from 1.06% to 7.4% under the conditions of an input peak power of 10 mW, a beam voltage of 9.55 kV and a current of 12 mA. The optimized MBFW structure can be successfully fabricated by micro milling, with dimension errors below expectation, and the measured transmission characteristics are in good agreement with the design.
    10  Multidimensional Co3O4 nano sponge for the highly sensitive SERS applications
    ZHAO Miao-miao LIU Wen-yao DU Jian-gong GUO Xu-dong WANG Lei XIA Mei-jing TANG Jun
    2017, 13(1):38-41. DOI: 10.1007/s11801-017-6236-1
    [Abstract](3904) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    In this work, surface enhanced Raman spectroscopy (SERS) substrates with Ag nanoparticles (NPs) decorated Co3O4 nanowires (NWs) grafted on the three-dimensional (3D) network architecture of Ni foam (denoted as Ag-NP@Co3O4- NW/Ni-foam) arrays are manufactured. In the experiment, the hierarchical Ag-NP@Co3O4-NW/Ni-foam arrays exhibit strong SERS activity due to the higher density of the “hot spots” created from the large quantities of neighboring Ag NPs. Using this hierarchical 3D SERS substrates, the crystal violet (a banned drug of aquaculture) with concentration down to 10-14 mol/L can be detected, which shows potential application in SERS-based rapid trace-level detection of harmful food additives.
    11  Effects of Mg doping content and annealing temperature on the structural properties of Zn1-xMgxO thin films prepared by radio-frequency magnetron sputtering
    DU Wen-han YANG Jing-jing ZHAO Yu XIONG Chao
    2017, 13(1):42-44. DOI: 10.1007/s11801-017-6204-9
    [Abstract](3899) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    The doping content of Mg plays an important role in the crystalline structure and morphology properties of Zn1-xMgxO thin films. Here, using radio-frequency magnetron sputtering method, we prepared Zn1-xMgxO thin films on single crystalline Si(100) substrates with a series of x values. By means of X-ray diffraction (XRD) and scanning electron microscope (SEM), the crystalline structure and morphology of Zn1-xMgxO thin films with different x values are investigated. The crystalline structure of Zn1-xMgxO thin film is single phase with x<0.3, while there is phase separation phenomenon with x>0.3, and hexagonal and cubic structures will coexist in Zn1-xMgxO thin films with higher x values. Especially with lower x values, a shoulder peak of 35.1° appearing in the XRD pattern indicates a double-crystalline structure of Zn1-xMgxO thin film. The crystalline quality has been improved and the inner stress has been released, after the Zn1-xMgxO thin films were annealed at 600 °C in vacuum condition.
    12  Effects of etching conditions on surface morphology of periodic inverted trapezoidal patterned Si(100) substrate
    ZHANG Lu YUAN Guo-dong WANG Qi WANG Ke-chao WU Rui-wei LIU Zhi-qiang LI Jin-min WANG Jun-xi
    2017, 13(1):45-49. DOI: 10.1007/s11801-017-6242-3
    [Abstract](3764) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    In this paper, the anisotropic etching process of Si(100) wafers in tetramethyl ammonium hydroxide (TMAH) solution with isopropyl alcohol (IPA) is investigated in detail. An inverted trapezoidal pattern is developed. A series of experiments are performed by changing TMAH concentration, IPA concentration, etching temperature and etching time. The structure of inverted trapezoidal patterns and roughness of the bottom surface are characterized by scanning electron microscopy (SEM) and atomic force microscopy (AFM). The results show that with TMAH concentration increases, the roughness of bottom surface will decrease. The addition of IPA into TMAH solution improves the morphology of the bottom surface significantly. Low temperature is beneficial to get a smooth bottom surface. Furthermore, etching time can change the bottom surface roughness. A model is proposed to explain the etching processes. The hillock area ratio of the bottom surface has the same tendency as the etching area ratio. Finally, smooth silicon inverted trapezoidal patterns are obtained for epitaxial growth of GaN-based light emitting diode (LED) devices.
    13  Preparation and laser properties of Yb3+-doped microstructure fiber based on hydrolysis-melting technique
    WANG Chao
    2017, 13(1):50-53. DOI: 10.1007/s11801-017-6257-9
    [Abstract](3715) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    The Yb3+-doped silica glass was prepared by the SiCl4 hydrolysis doping and powder melting technology based on high frequency plasma. The absorption and emission characteristics of the Yb3+-doped silica glass are studied at room temperature. The integrated absorption cross section, stimulated emission cross section and fluorescence lifetime are calculated to be 8.56×104 pm3, 1.39 pm2 and 0.56 ms, respectively. The Yb3+-doped microstructure fiber (MSF) was also fabricated by using the Yb3+-doped silica glass as fiber core. What’s more, the laser properties of the Yb3+-doped MSF are studied.
    14  Enhanced 1.32 µm fluorescence and broadband amplifying for O-band optical amplifier in Nd3+-doped tellurite glass
    ZHOU Zi-zhong ZHOU Ming-han SU Xiu-e CHENG Pan ZHOU Ya-xun
    2017, 13(1):54-57. DOI: 10.1007/s11801-017-6260-1
    [Abstract](3788) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    WO3 oxides with relatively high phonon energy and different concentrations were introduced into the Nd3+-doped tellurite-based glasses of TeO2-ZnO-Na2O to improve the 1.32 µm band fluorescence emission. The absorption spectra, Raman spectra, 1.32 µm band fluorescence spectra and differential scanning calorimeter (DSC) curves were measured, together with the Judd-Ofelt intensity parameters, stimulated emission and gain parameters were calculated to evaluate the effects of WO3 amount on the glass structure and spectroscopic properties of 1.32 µm band fluorescence. It is shown that the introduction of an appropriate amount of WO3 oxide can effectively improve the 1.32 µm band fluorescence intensity through the enhanced multi-phonon relaxation (MPR) processes between the excited levels of Nd3+. The results indicate that the prepared Nd3+-doped tellurite glass with an appropriate amount of WO3 oxide is a potential gain medium applied for the O-band broad and high-gain fiber amplifier.
    15  Realization of OFDM modulation and demodulation for visible light communication based on FPGA
    WU Chun-hui GAO Zong-yu LI Hong-lei CHEN Xiong-bin MAO Xu-rui LU Hui-min WANG Jian-ping HE Lin CUI Shi-gang CHEN Hong-da
    2017, 13(1):58-62. DOI: 10.1007/s11801-017-6233-4
    [Abstract](4228) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    In order to ensure stable, correct and real-time high-speed transmission of indoor visible light communication (VLC), the key modulation and demodulation technologies of orthogonal frequency division multiplexing (OFDM) are studied in this paper. The time-domain synchronization, frequency synchronization and channel equalization of receiver are analyzed and optimized by utilizing short and long training preamble. Moreover, field programmable gate array (FPGA) development board (Xilinx Kintex-7) and Verilog hardware description language are used to realize the design of proposed OFDM-VLC system. Simulation and experiment both verify the feasibility of the hardware designs of this system. The proposed OFDM-based VLC system can process signal in real-time, which can be used in actual VLC application systems.
    16  Study on RZ-4PAM downstream signals with duty cycles of 33% and 50% for optical access system application
    CHEN Fu-ping SHAO Yu-feng CHEN Lao SHEN Shi-lu WANG An-rong LUO Ying-xiang ZHAO Yun-jie
    2017, 13(1):63-66. DOI: 10.1007/s11801-017-6197-4
    [Abstract](3755) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    4-ary pulse amplitude modulation (4PAM) signals with 33% and 50% return-to-zero (RZ) clocks are generated for passive optical network (PON). We demonstrate that RZ-4PAM signals with duty cycles of 33% and 50% after transmission over 20-km-long single mode fiber (SMF) at 10 Gbit/s can be directly detected by using one photo detector, and the original data can also be restored by one M-ary threshold detector and one 4PAM sequence decoder. The optical spectra of 33% and 50% RZ-4PAM signals are measured, and their eye-diagrams before and after transmission are also analyzed. Simulation results show that 33% and 50% RZ-4PAM downlink signals can be received effectively, and the received power values are −15.1 dBm and −13.8 dBm when the bit error rate (BER) is 10-6. Moreover, 33% RZ-4PAM optical signals have better reception performance than 50% RZ-4PAM optical signals.
    17  A WDM-PON with DPSK modulated downstream and OOK modulated upstream signals based on symmetric 10 Gbit/s wavelength reused bidirectional reflective SOA
    2017, 13(1):67-69. DOI: 10.1007/s11801-017-6227-2
    [Abstract](3665) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    We investigate a wavelength-division-multiplexing passive optical network (WDM-PON) with centralized lightwave and direct detection. The system is demonstrated for symmetric 10 Gbit/s differential phase-shift keying (DPSK) downstream signals and on-off keying (OOK) upstream signals, respectively. A wavelength reused scheme is employed to carry the upstream data by using a reflective semiconductor optical amplifier (RSOA) as an intensity modulator at the optical network unit (ONU). The constant-intensity property of the DPSK modulation format can keep high extinction ratio (ER) of downstream signal and reduce the crosstalk to the upstream signal. The bit error rate (BER) performance of our scheme shows that the proposed 10 Gbit/s symmetric WDM-PON can achieve error free transmission over 25-km-long fiber transmission with low power penalty.
    18  Three-dimensional measurement of bubble volume based on dual perspective imaging
    XUE Ting ZHANG Shao-jie WU Bin
    2017, 13(1):70-73. DOI: 10.1007/s11801-017-6251-2
    [Abstract](3869) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    This paper presents a new three-dimensional (3D) volume measurement approach of bubble in gas-liquid two-phase flow. According to the dual perspective imaging principle, bubble feature images can be captured from two different view angles. The least square ellipse fitting algorithm is used to figure out the feature parameters from the captured images. Then the 3D volume of bubble can be quantitatively measured. Compaerd with the traditional volume estimation methods based on single perspective imaging, it can effectively reduce the loss of bubble feature information. In the experiment, the 3D volume reconstruction of bubbles from dual perspective images is conducted, and the variation of bubble volume in the bubble rising process is studied. The results show that the measurement accuracy based on the proposed 3D method is higher than those based on traditional methods. The volume of rising bubble is periodically changed, which indicates that bubble achieves periodic rotation and deformation in the rising process.
    19  Experimental simulation of spin-1 states by second-order type-II parametric down-conversion
    ZHAO Jia-qiang CAO Lian-zhen YANG Yang LU Huai-xin
    2017, 13(1):74-76. DOI: 10.1007/s11801-017-6234-3
    [Abstract](3811) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    In this paper, by using the second-order parametric down-conversion of the nonlinear crystal, the spin-1 state is simulated by the two-photon polarization entangled modes. Through adjusting the laser pulse power density, the efficiency of second-order parametric down-conversion is enhanced. The intensity of the spin-1 state is 0.5/s. The fidelity of the state is up to F=0.891±0.002, and the contrast is C=17.3. The results provide a new method for Stern-Gerlach measurement on the spin-1 system.
    20  Study on the echinococcosis blood serum detection based on Raman spectroscopy combined with neural network
    CHENG Jin-ying XU Liang Lü Guo-dong TANG Jun MO Jia-qing Lü Xiao-yi GAO Zhi-xian
    2017, 13(1):77-78. DOI: 10.1007/s11801-017-6259-7
    [Abstract](3877) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    A Raman spectroscopy method combined with neural network is used for the invasive and rapid detection of echinococcosis. The Raman spectroscopy measurements are performed on two groups of blood serum samples, which are from 28 echinococcosis patients and 38 healthy persons, respectively. The normalized Raman reflection spectra show that the reflectivity of the echinococcosis blood serum is higher than that of the normal human blood serum in the wavelength ranges of 101—175 nm and 1 801—2 701 nm. Then the principal component analysis (PCA) and back propagation neural network (BPNN) model are used to obtain the diagnosis results. The diagnosis rates for healthy persons and echinococcosis persons are 93.333 3% and 90.909 1%, respectively, so the average final diagnosis rate is 92.121 2%. The results demonstrate that the Raman spectroscopy analysis of blood serum combined with PCA-BPNN has considerable potential for the non-invasive and rapid detection of echinococcosis.